Published in
Royal Society of Chemistry, Organic and Biomolecular Chemistry, 44(15), p. 9372-9378, 2017
DOI: 10.1039/c7ob01995e
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NMR-based assignment of isoleucine vs. allo-isoleucine stereochemistry
Journal article published in 2017 by
Zoe J. Anderson,
Christian Hobson,
Rebecca Needley,
Lijiang Song,
Michael S. Perryman,
Paul Kerby,
David J. Fox 
This paper is made freely available by the publisher.
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Abstract
A simple1H and13C NMR spectrometric analysis is demonstrated that permits differentiation of isoleucine andallo-isoleucine residues by inspection of the chemical shift and coupling constants of the signals associated with the proton and carbon at the α-stereocentre.