Published in
Royal Society of Chemistry, Dalton Transactions, 22(46), p. 7223-7231, 2017
DOI: 10.1039/c7dt01019b
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Solvent-dependent nuclearity, geometry and catalytic activity of [(SPhos)Pd(Ph)Cl]2
Journal article published in 2017 by
John B. Brazier,
Mark A. Newton,
Elena M. Barreiro 
,
Luis A. Adrio ,
Leticia Naya ,
King Kuok (Mimi) Hii
,
Luis A. Adrio ,
Leticia Naya ,
King Kuok (Mimi) Hii
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Abstract
The nuclearity and structures of the palladium complex [(SPhos)Pd(Ph)Cl]2 in the solid and solution states are revisited using a combination of Extended X-ray Absorption Fine Structure (EXAFS) spectroscopy, NMR spectroscopy, mass spectrometry, DFT calculations and trapping experiments.