Published in
Royal Society of Chemistry, Chemical Communications, 25(46), p. 4514
DOI: 10.1039/b924936b
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On-line monitoring of a microwave-assisted chemical reaction by nanolitre NMR-spectroscopy
Journal article published in 2010 by
M. Victoria Gomez,
M. Victoria Gomez,
Hein H. J. Verputten,
Angel Díaz-Ortíz,
Andres Moreno,
Antonio de la Hoz 
,
Aldrik H. Velders
,
Aldrik H. Velders
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Abstract
We report the use of a nanolitre nuclear magnetic resonance (NMR) spectroscopy microfluidic chip hyphenated to a continuous-flow microlitre-microwave irradiation set-up, for on-line monitoring and rapid optimization of reaction conditions.