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Royal Society of Chemistry, Chemical Communications, 84(51), p. 15410-15413

DOI: 10.1039/c5cc06293d

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Measuring Couplings in Crowded NMR Spectra: Pure Shift NMR with Multiplet Analysis

Journal article published in 2015 by Mohammadali Foroozandeh, Ralph W. Adams ORCID, Peter Kiraly, Mathias Nilsson, Gareth A. Morris
This paper is made freely available by the publisher.
This paper is made freely available by the publisher.

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Abstract

The PSYCHE method for pure shift NMR is exploited to generate 2D J spectra with full decoupling in one dimension and multiplet structure in the other, allowing spin-spin coupling constants to be measured even in very crowded spectra. Significant improvements over existing techniques are demonstrated for the hormones estradiol and androstenedione.