Published in
Royal Society of Chemistry, Chemical Communications, 12, p. 1307
DOI: 10.1039/b517812f
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TEMPO-mediated, room temperature synthesis of pure CoO nanoparticles
Journal article published in 2006 by
Anna Lagunas,
Antoni Mairata I. Payeras,
Ciril Jimeno,
Miquel A. Pericàs 
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Abstract
Treatment of dicobalt octacarbonyl with TEMPO in THF at room temperature, in the presence of oleic acid as the sole additive, leads to the formation of monodisperse nanoparticles (ca. 3.0 nm diameter) of CoO; the particles agglomerate in solution at room temperature into aggregates, and this property has been used for the controlled preparation of hybrid materials.