Published in
Royal Society of Chemistry, Analyst, 6(140), p. 1804-1808
DOI: 10.1039/c4an02248c
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En route to traceable reference standards for surface group quantifications by XPS, NMR and fluorescence spectroscopy
Journal article published in 2015 by
Andreas Hennig,
Paul M. Dietrich 
,
Felix Hemmann,
Thomas Thiele,
Heike Borcherding,
Angelika Hoffmann,
Uwe Schedler,
Christian Jäger,
Ute Resch-Genger,
Wolfgang E. S. Unger
,
Felix Hemmann,
Thomas Thiele,
Heike Borcherding,
Angelika Hoffmann,
Uwe Schedler,
Christian Jäger,
Ute Resch-Genger,
Wolfgang E. S. Unger
This paper is made freely available by the publisher.
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Abstract
The fluorine content of polymer particles labelled with 2,2,2-trifluoroethylamine was reliably quantified with overlapping sensitivity ranges by XPS and solid-state NMR. This provides a first step towards reference materials for the metrological traceability of surface group quantifications. The extension of this concept to fluorescence spectroscopy is illustrated.