Published in
Royal Society of Chemistry, Dalton Transactions, 4, p. 433-436
DOI: 10.1039/b714274a
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The preparation and characterisation of ruthenium cyanovinylidene complexes
Journal article published in 2008 by
Neil J. Brown,
Prisca K. Eckert,
Mark A. Fox 
,
Dmitri S. Yufit,
Judith A. K. Howard,
Paul J. Low
,
Dmitri S. Yufit,
Judith A. K. Howard,
Paul J. Low
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Abstract
Reactions of half-sandwich ruthenium metal acetylide complexes with 1-cyano-4-dimethylaminopyridinium salts afford complexes containing mono- or di-cyanovinylidene ligands; the procedure can be adapted to permit the simple synthesis of a cyanoacetylide complex, via the in situ deprotonation of a primary cyanovinylidene complex.