Published in
Royal Society of Chemistry, Chemical Communications, 52(51), p. 10419-10422, 2015
DOI: 10.1039/c5cc03102h
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One-pot tandem catalysis over Pd@MIL-101: boosting the efficiency of nitro compound hydrogenation by coupling with ammonia borane dehydrogenation
Journal article published in 2015 by
Qihao Yang,
Yu-Zhen Chen,
Zhiyong U. Wang,
Qiang Xu 
,
Hai-Long Jiang
,
Hai-Long Jiang
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Abstract
The hydrogenation efficiency of nitro compounds was found to be greatly boosted by coupling with dehydrogenation of ammonia borane. The Pd@MIL-101 with tiny Pd NPs is exceptionally efficient and recyclable in the tandem reactions and diverse nitro compounds can be selectively reduced to the corresponding amines in 1.5-5 min with quantitative yields.