Published in
Royal Society of Chemistry, Chemical Communications, 9(48), p. 1260-1262
DOI: 10.1039/c2cc16327f
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Palladium-catalysed direct arylation of a tris-cyclometallated Ir(III) complex bearing 2,2′-thienylpyridine ligands: a powerful tool for the tuning of luminescence properties
Journal article published in 2012 by
Kassem Beydoun,
Moussa Zaarour,
J. A. G. Williams,
J. A. Gareth Williams,
J. A. Gareth Williams,
Henri Doucet,
Véronique Guerchais 
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Abstract
Palladium-catalysed direct 5-arylation of metallated thiophenes of fac-Ir(N^C(3')-thpy)(3) with aryl bromides via C-H bond functionalisation allows the synthesis of a variety of new Ir complexes in only one step (thpyH = 2,2'-thienylpyridine). The method offers simple modification of the nature of the ligand and hence of the photophysical properties of such complexes.