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Royal Society of Chemistry, Physical Chemistry Chemical Physics, 40(23), p. 22912-22922, 2021

DOI: 10.1039/d1cp03320d

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Two-bond <sup>13</sup>C–<sup>13</sup>C spin-coupling constants in saccharides: dependencies on exocyclic hydroxyl group conformation

Journal article published in 2021 by Jieye Lin ORCID, Reagan J. Meredith, Allen G. Oliver ORCID, Ian Carmichael ORCID, Anthony S. Serianni ORCID
This paper is made freely available by the publisher.
This paper is made freely available by the publisher.

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Abstract

13C-Labeled mono- and disaccharides were studied by X-ray crystallography and solid-state 13C NMR to determine the dependence of 2JC1,C3 in aldopyranosyl rings on the C1–C2–O2–H torsion angle, θ2, involving C2 of the C1–C2–C3 coupling pathway.