Published in
Royal Society of Chemistry, Organic and Biomolecular Chemistry, 10(21), p. 2118-2126, 2023
DOI: 10.1039/d2ob02160a
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Practical synthesis and biological screening of sulfonyl hydrazides
Journal article published in 2023 by
João Macara,
Catarina Caldeira,
José Cunha 
,
Jaime A. S. Coelho ,
Maria J. S. A. Silva ,
Konrad Krämer,
Christoph W. Grathwol,
Stefan Bräse,
M. Manuel B. Marques
,
Jaime A. S. Coelho ,
Maria J. S. A. Silva ,
Konrad Krämer,
Christoph W. Grathwol,
Stefan Bräse,
M. Manuel B. Marques
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Abstract
A hypervalent iodine-mediated synthesis of sulfonyl hydrazides is described. The methodology relies on the umpolung reactivity of benziodoxolone reagents. Mechanistic studies and biological screening were performed.