Published in
Royal Society of Chemistry, Physical Chemistry Chemical Physics, 41(24), p. 25279-25286, 2022
DOI: 10.1039/d2cp02872g
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Investigating the efficiency of silica materials with wall-embedded nitroxide radicals for dynamic nuclear polarisation NMR
Journal article published in 2022 by
Eric Besson,
Aurelien Vebr,
Fabio Ziarelli,
Emily Bloch,
Guillaume Gerbaud 
,
Séverine Queyroy,
Pierre Thureau ,
Stéphane Viel ,
Stéphane Gastaldi
,
Séverine Queyroy,
Pierre Thureau ,
Stéphane Viel ,
Stéphane Gastaldi
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Abstract
A wide range of mesoporous silicas functionalized with face-to-face TEMPO at a controlled distance has been studied as polarizing agents for DNP NMR. Their enhancement factors yield promising systems for various future applications.