Published in
Royal Society of Chemistry, Faraday Discussions, (229), p. 422-442, 2021
DOI: 10.1039/c9fd00145j
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Multi-Nuclear, High-pressure, Operando FlowNMR Spectroscopic Study of Rh/PPh3 - Catalysed Hydroformylation of 1-Hexene
Journal article published in 2020 by
Alejandro Bara-Estaun 
,
Catherine L. Lyall ,
John P. Lowe,
Paul G. Pringle ,
Paul C. J. Kamer ,
Robert Franke,
Ulrich Hintermair
,
Catherine L. Lyall ,
John P. Lowe,
Paul G. Pringle ,
Paul C. J. Kamer ,
Robert Franke,
Ulrich Hintermair
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Abstract
The hydroformylation of 1-hexene with 12 bar of 1 : 1 H2/CO in the presence of the catalytic system [Rh(acac)(CO)2]/PPh3 was successfully studied by real-time multinuclear high-resolution FlowNMR spectroscopy at 50 °C.