Published in
Royal Society of Chemistry, Organic and Biomolecular Chemistry, 38(17), p. 8701-8705, 2019
DOI: 10.1039/c9ob01758e
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One-pot synthesis of high molar activity 6-[18F]fluoro-l-DOPA by Cu-mediated fluorination of a BPin precursor
Journal article published in 2019 by
Andrew V. Mossine 
,
Sean S. Tanzey ,
Allen F. Brooks ,
Katarina J. Makaravage ,
Naoko Ichiishi ,
Jason M. Miller,
Bradford D. Henderson,
Marc B. Skaddan,
Melanie S. Sanford ,
Peter J. H. Scott
,
Sean S. Tanzey ,
Allen F. Brooks ,
Katarina J. Makaravage ,
Naoko Ichiishi ,
Jason M. Miller,
Bradford D. Henderson,
Marc B. Skaddan,
Melanie S. Sanford ,
Peter J. H. Scott
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Abstract
A one-pot two-step synthesis of 6-[18F]fluoro-l-DOPA has been developed, involving Cu-mediated radiofluorination of the corresponding pinacol boronate ester precursor, and validated for production of doses for human use.