Published in
Royal Society of Chemistry, Chemical Communications, 64(55), p. 9523-9526, 2019
DOI: 10.1039/c9cc03316e
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Unexpected linkage isomerism in chiral tetranuclear bis-tridentate (1,2,3-triazol-4-yl)-picolinamide (tzpa) grids
Journal article published in 2019 by
Isabel N. Hegarty,
Hannah L. Dalton,
Adam F. Henwood,
Chris S. Hawes 
,
Thorfinnur Gunnlaugsson
,
Thorfinnur Gunnlaugsson
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Abstract
Two chiral [2 × 2] tetranuclear CuII square grid complexes are prepared from a (1,2,3-triazol-4-yl)-picolinamide (tzpa) ligand. Linkage isomerism through the amide is observed accompanying an in situ deprotonation and CuI → CuII oxidation process.