Fe(ii) and Fe(iii) dithiocarbamate complexes as single source precursors to nanoscale iron sulfides: a combined synthetic and in situ XAS approach
Journal article published in 2019 by
Anna Roffey 
,
Nathan Hollingsworth,
Husn-Ubayda Islam,
Wim Bras ,
Gopinathan Sankar,
Nora H. de Leeuw ,
Graeme Hogarth
,
Nathan Hollingsworth,
Husn-Ubayda Islam,
Wim Bras ,
Gopinathan Sankar,
Nora H. de Leeuw ,
Graeme Hogarth
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Abstract
Fe(ii) and Fe(iii) dithiocarbamates are precursors to a range of nanoparticulate iron sulfides and in situ studies give insight into the molecular decomposition mechanism being dominated by reductive-elimination of thiuram disulfide and amide-exchange.