Published in
Royal Society of Chemistry, Dalton Transactions, 17(48), p. 5520-5522, 2019
DOI: 10.1039/c9dt00953a
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Phosphine-promoted ring-opening of benzisothiazolinate ligands at a nickel(ii) centre: a convenient synthesis of Ni(ii)-thiolate complexes
Journal article published in 2019 by
Subhi A. Al-Jibori,
Samer Hussein Ali,
Ahmed S. Al-Janabi 
,
Christoph Wagner,
Graeme Hogarth
,
Christoph Wagner,
Graeme Hogarth
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Abstract
Phosphines react with the benzisothiazolinate (bit) paddlewheel dimer, [Ni2(μ-bit)4·2H2O], resulting in sulfur–nitrogen bond scission and a series of unexpected transformations leading to novel Ni(ii) complexes containing 2-cyanophenylthiolate and related thiolate ligands.