Published in
Royal Society of Chemistry, Dalton Transactions, 14(46), p. 4737-4748
DOI: 10.1039/c7dt00305f
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Formation of paramagnetic metallacyclobutadienes by reaction of diaminoacetylenes with molybdenum alkylidyne complexes
Journal article published in 2017 by
Òscar Àrias 
,
Kai Brandhorst ,
Dirk Baabe,
Matthias Freytag,
Peter G. Jones,
Matthias Tamm
,
Kai Brandhorst ,
Dirk Baabe,
Matthias Freytag,
Peter G. Jones,
Matthias Tamm
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Abstract
The reactions of the molybdenum alkylidyne complex [MesCMo{OCMe(CF3)2}3] with the diaminoacetylenes R2NCCNR2 (NR2 = 4-methylpiperidinyl, NEt2; Mes = 2,4,6-trimethylphenyl) afforded paramagnetic metallacyclobutadiene (MCBD) complexes with diaminodicarbene ligands.