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De Gruyter, Zeitschrift für Naturforschung B, 11(58), p. 1133-1140, 2003

DOI: 10.1515/znb-2003-1117

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Synthesis and Spectroscopy of LiClO4 Complexes of (-)-Sparteine, 2-Methyl- and 2-Oxosparteine, and 2-Cyano-2-methylsparteine

Journal article published in 2003 by Beata Jasiewicz, Tomasz Rafałowicz, Ewa Sikorska, Igor Khmelinskii ORCID, Jacek Koput, Marek Sikorski, Władysław Boczoń
This paper was not found in any repository, but could be made available legally by the author.
This paper was not found in any repository, but could be made available legally by the author.

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Abstract

Complexes formed between (-)-sparteine, 2-methyl- and 2-oxosparteine and 2-cyano-2- methylsparteine with lithium perchlorate (LiClO4) were obtained in the solid state. The complexes, C15H26N2LiClO4, C16H28N2LiClO4, C15H24N2OLiClO4, and C17H27N3Li2Cl2O8 have been isolated and characterised by UV/vis, NMR, and IR, spectroscopy and by their mass spectra. Three of the four complexes present the 1:1 stoichiometry, while the 2-cyano-2-methylsparteine complex has the 1:2 stoichiometry.