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American Chemical Society, Journal of the American Chemical Society, 36(129), p. 10972-10973, 2007

DOI: 10.1021/ja0721115

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Residual dipolar couplings by off-magic-angle spinning in solid-state nuclear magnetic resonance spectroscopy

Journal article published in 2007 by Giuseppe Pileio, Ying Guo, Tran N. Pham, John M. Griffin, Malcolm H. Levitt ORCID, Steven P. Brown
This paper is available in a repository.
This paper is available in a repository.

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Abstract

A solid-state NMR analogue of the solution-state residual dipolar coupling effect is demonstrated. A small misset of the spinning axis by less than 0.5 degrees changes the modulation frequency of spin-echoes, allowing the estimation of internuclear dipole-dipole couplings and hence internuclear distances.