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Serbian Chemical Society, Journal of the Serbian Chemical Society, 12(81), p. 1383-1392, 2016

DOI: 10.2298/jsc160915087s

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Synthesis and characterization of palladium(II) complexes with glycine coumarin derivatives

Journal article published in 2016 by Danijela Stojkovic, Alessia Bacchi, Davide Capucci, Milica Milenkovic ORCID, Bozidar Cobeljic ORCID, Srecko Trifunovic ORCID, Katarina Andjelkovic, Verica Jevtic ORCID, Nenad Vukovic ORCID, Milena Vukic ORCID, Dusan Sladic ORCID
This paper is made freely available by the publisher.
This paper is made freely available by the publisher.

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Abstract

A Pd(II) complex with methyl 2-((1-(2,4-dioxochroman-3-ylidene)ethyl)amino)acetate was synthesized. The structures of both the ligand and Pd(II) complex were determined by elemental analysis, IR and NMR spectroscopy. Recrystallization of Pd(II) complex from DMF/water solution resulted in its hydrolysis and formation of dimethylamine-(2-((1-(2,4-dioxochroman-3-ylidene)ethyl)amino)acetato)palladium(II) complex, the structure of which was determined by elemental analysis, IR, 1H and 13C NMR spectroscopy, as well as X-ray analysis.