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Trans Tech Publications, Advanced Materials Research, (833), p. 169-172, 2013

DOI: 10.4028/www.scientific.net/amr.833.169

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Effect of Solid Loading on Properties of All-Ceramic Crown by Gel-Casting Technique

Journal article published in 2013 by Peng Zhang, Hong Yu Guan
This paper was not found in any repository, but could be made available legally by the author.
This paper was not found in any repository, but could be made available legally by the author.

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Abstract

To compare the influence of porosity on bending strength, density, viscosity of slurry of dental zirconia-toughened alumina(Ce-TZP/A) ceramic by gel-casting technique. Ce-TZP/A composite ceramic powder was made from a Al2O3 of micron grade and 3Ce-ZrO2 of nanometer grade, with sintering additives of MgO and TiO2. The slurries of 5(v/v), 52%, 54%, 56% ,58% and 60% were prepared separately, and sintered at 1200°C after in situ molding using gel-casting. The properties such as bending strength, density, viscosity of slurry of specimens were measure and compared. Slurry was prepared with optimum solid content, and applied to form dental CeTZP/A basal crown on the plaster die. The marginal fitness of crowns was observed after sintered. The mean viscosity of slurry (PaS) were: 0.27±0.05, 0.31±0.1, 0.33±0.09, 0.96±0.12, 1.01±0.07, 1.21±0.02. The effect of solid loading (P=0.05) were significant. The mean bending strength (MPa) were: 43.15±0.8, 47.9±1.5, 50.09±1.7, 58.12±1.9, 39.17±1.6, 35.08±1.2. The mean toughness (MPa m^1/2) were: 17.6±0.8, 16.9±0.6, 16.1±0.5, 17.8±0.9, 18.6±0.8, 20.5±0.2. The mean density (g/cm) were: 5.32±0.9, 5.43±0.8, 6.13±0.5, 6.01±0.5, 5.13±0.3, 5.05±0.4. The specimen formed from slurry of 52(v/v) had better properties than that of others solid loading after sintered at 1150º. With the solid loading increased, the viscosity of slurry has a significantly improved.