Online monitoring of heterogeneous polymerizations in supercritical carbon dioxide by Raman spectroscopy
Journal article published in 2012 by
Bruno Grignard 
,
Bernard Gilbert,
Cédric Malherbe,
Christine Jérôme,
Christophe Detrembleur
,
Bernard Gilbert,
Cédric Malherbe,
Christine Jérôme,
Christophe Detrembleur
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Abstract
A novel setup is described to monitor the kinetics of homogeneous and heterogeneous reactions online using Raman spectroscopy under high pressure. The arrangement is based on a high-pressure reactor equipped with a sapphire window in combination with a mobile probe that allows the collection of the back-scattered Raman signal at 360°.