Published in

Wiley, Journal of the American Ceramic Society, 12(98), p. 3639-3642, 2015

DOI: 10.1111/jace.13945

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Microtexture Analysis of the Alumina Scale in Thermal Barrier Coatings

This paper was not found in any repository, but could be made available legally by the author.
This paper was not found in any repository, but could be made available legally by the author.

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Abstract

Transmission electron microscopy-based grain orientation map-ping method was employed to investigate the microtexture of the alumina scale formed in commercial thermal barrier coat-ings (TBCs) with two standard types of Pt-enriched bond coats. Reliable orientation/phase maps with a spatial resolution down to 2 nm were acquired on the alumina grains. It was observed that the alumina scale on the Pt-aluminide b-phase bond coat has a stronger c-axis texture normal to the bond coat surface, in comparison with that on the Pt-diffused c/c0-phase bond coat. The microtexture of the alumina scale could affect its effective coefficient of thermal expansion, which is a contributor to the severity of the bond coat rumpling mecha-nism of TBCs failure.