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Institute of Electrical and Electronics Engineers, IEEE Transactions on Magnetics, 11(51), p. 1-4, 2015

DOI: 10.1109/tmag.2015.2442457

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Formation of Magnetic Nanoparticles by Annealing Continuous CoFeB/Cu Bilayer Thin Films

Journal article published in 2015 by Ting Xie ORCID, Romel D. Gomez
This paper is available in a repository.
This paper is available in a repository.

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Abstract

This paper reports a novel yet simple mask-less method for fabricating monodisperse submicron magnetic islands by annealing continuous CoFeB/Cu bilayer films. Annealing drives the diffusion of Co and Fe into the Cu under-layer, causing them to aggregate into submicron islands at the Cu grain boundaries. This was established by in-situ Auger electron spectroscopy, along with scanning electron microscopy (SEM), high-resolution atomic and magnetic force microscopy to determine the surface composition at various stages of preparation. The composition of the magnetic clusters was established by energy dispersive x-ray spectroscopy (EDS). Our results indicate that Co and Fe are coalesced with their relative ratio remaining similar to the starting composition of the sputtering target, while boron is dissociated from the magnetic species. Also, the areal density of the islands was found to be strongly dependent on the Cu thickness and annealing temperature, while the size of magnetic particles was only weakly dependent. This feature was utilized to control the distribution of monosized magnetic islands.