Published in

Elsevier, Journal of Magnetic Resonance, 1(213), p. 196-199

DOI: 10.1016/j.jmr.2011.09.015

Links

Tools

Export citation

Search in Google Scholar

An efficient amplification pulse sequence for measuring chemical shift anisotropy under fast magic-angle spinning

Journal article published in 2011 by Ivan Hung ORCID, Zhehong Gan
This paper was not found in any repository, but could be made available legally by the author.
This paper was not found in any repository, but could be made available legally by the author.

Full text: Unavailable

Green circle
Preprint: archiving allowed
Red circle
Postprint: archiving forbidden
Red circle
Published version: archiving forbidden
Data provided by SHERPA/RoMEO

Abstract

A two-dimensional experiment for measuring chemical shift anisotropy (CSA) under fast magic-angle spinning (MAS) is presented. The chemical shift anisotropy evolution is amplified by a sequence of π-pulses that repetitively interrupt MAS averaging. The amplification generates spinning sideband manifolds in the indirect dimension separated by the isotropic shift along the direct dimension. The basic unit of the pulse sequence is designed based on the magic-angle turning experiment and can be concatenated for larger amplification factors.