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Trans Tech Publications, Key Engineering Materials, (264-268), p. 133-136, 2004

DOI: 10.4028/www.scientific.net/kem.264-268.133

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Low Temperature Rapid Synthesis of Spinel Lithium Manganese Oxide Fine Particles by Microwave Heating

Journal article published in 2004 by A. Ahniyaz ORCID, T. Fujiwara, Hao Wang, M. Yoshimura
This paper is available in a repository.
This paper is available in a repository.

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Abstract

Spinel LiMn2O4 was successfully prepd. at a low temp. rapidly by microwave heating method. LiMn2O4 fine particles can be easily prepd. in a few minutes by microwave heating of g-MnOOH powders in a LiOH + H2O2 soln. This prepn. process can provide an efficient, economical, and environmentally friendly way of prepn. of LiMn2O4. The spinel LiMn2O4 phase formation was confirmed by XRD, XPS, TG-DTA, and SEM