Detrital zircon grains from Lower Paleozoic sedimentary rocks in the Yucatan Peninsula have an age distribution characterized by major probability peaks at ~ 1.0, ~ 1.2, and ~ 1.5 Ga (Martens et al., 2010). Here, we present new Lu–Hf data (MC–ICPMS) paired with U–Pb ages (ID-TIMS) for additional zircon grains from the same rocks. This analytical approach yields precise information about the time and geochemical environment of zircon growth, which in turn helps to distinguish between different crustal source regions that just happen to host zircon populations of similar age. In addition, single zircon grains from granitoids that intruded the sedimentary rocks were dated by U–Pb laser ablation MC–ICPMS and ID-TIMS, and their Hf-isotope compositions were determined by solution MC–ICPMS. The zircon data are complemented by Sm–Nd analyses of the sedimentary and igneous whole rocks.