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Trans Tech Publications, Materials Science Forum, (715-716), p. 486-491, 2012

DOI: 10.4028/www.scientific.net/msf.715-716.486

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EBSD Coupled to SEM <i>In Situ</i> Annealing as a Tool to Identify Recrystallization Mechanisms - Application to Zr and Ta Alloys

Journal article published in 2012 by Nathalie Bozzolo, S. Jacomet, M. Houillon, B. Gaudout, Roland E. Logé ORCID
This paper is made freely available by the publisher.
This paper is made freely available by the publisher.

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Abstract

A heating stage as been developed to performin-situannealing in a SEM equipped with an EBSD system in order to study recrystallization mechanisms. High temperature treatments could then be performed inside the SEM, up to 1180°C and with high heating-and cooling-rates (~100°C.s-1). Samples were cooled down to room temperature to perform EBSD orientation mapping in between successive short-duration heat-treatments. Microstructure evolution snapshots obtained this way are presented in this paper to show recrystallization in Zircaloy4 and in pure tantalum.