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Elsevier, Solid State Sciences, (42), p. 14-19, 2015

DOI: 10.1016/j.solidstatesciences.2015.03.003

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Hydroflux synthesis and crystal structure of new lanthanide tungstate oxyhydroxides

This paper was not found in any repository, but could be made available legally by the author.
This paper was not found in any repository, but could be made available legally by the author.

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Abstract

Single crystals of Na5Ln(OH)6WO4 where Ln Combining double low line Er, Tm, and Yb were grown out of a NaOH hydroflux. The crystals were characterized by single crystal X-ray diffraction and were found to crystallize in the monoclinic space group I2/a. The lattice parameter ranges for the three structures are a Combining double low line 11.2024(7),-11.2412(6) , b Combining double low line 16.1850(10) ,-16.2220(10) , and c Combining double low line 11.9913(7) ,-12.0323(7) , while the 2 angle range is 101.999(2)°-102.025(2)°.