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Facultad de Humanidades y Ciencias de la Educación, Synthesis: Journal of Synthetic Organic Chemistry, 04(2012), p. 635-647

DOI: 10.1055/s-0031-1289676

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Scale-Up of Flow-Assisted Synthesis of C2-Symmetric Chiral PyBox Ligands

Journal article published in 2012 by Claudio Battilocchio, Claudio Baumann, Marcus Baumann, Rainer E. Martin, Marcus Baxendale, Ian R. Baxendale, R. Ian, Mariangela Biava, Matthew O. Kitching ORCID, Steven V. Ley, Stephan A. Ohnmacht, Nicholas D. C. Tappin ORCID
This paper is made freely available by the publisher.
This paper is made freely available by the publisher.

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Abstract

A series of PyBox ligands were prepared from commercially available chelidonic acid by a multistep flow sequence using mesoreactor technology. A chloro group introduced onto the ligand scaffold was subsequently exploited to give amine derivatives ready for immobilization through microencapsulation technologies.