Published in
American Chemical Society, Journal of Organic Chemistry, 2(72), p. 643-646, 2006
DOI: 10.1021/jo0620866
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Seven-Membered Cyclic Sulfite Eudesmane Derivatives: Partial Synthesis, Structural Determination, and Enzymatic Resolution
Journal article published in 2007 by
Andrés García-Granados,
Andrés Parra,
Francisco Rivas 
,
Alejandro J. Segovia
,
Alejandro J. Segovia
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Abstract
Two chromatographically inseparable, diastereomeric eudesmane cyclic sulfites have been semisynthesized from alpha-santonin. This diastereomeric mixture was resolved by enzymatic acetylation with CCL. Each cyclic sulfite derivative was individually characterized on the basis of its spectroscopic and crystallographic properties.