Published in
Elsevier, Journal of Organometallic Chemistry, 1-2(658), p. 62-70
DOI: 10.1016/s0022-328x(02)01623-6
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Late transition metal complexes bearing 2,9-bis(imino)-1,10-phenanthrolinyl ligands: Synthesis, characterization and their ethylene activity
Journal article published in 2002 by
Leyong Wang 
,
Wen-Hua Sun ,
Lingqin Han,
Haijian Yang,
Youliang Hu,
Xianglin Jin
,
Wen-Hua Sun ,
Lingqin Han,
Haijian Yang,
Youliang Hu,
Xianglin Jin
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Abstract
A series of iron, cobalt and nickel halide complexes, LMX2 (M=Fe, X=Cl; M=Co, X=Cl; M=Ni, X=Br) bearing 2,9-bis(imino)-1,10-phenanthrolinyl ligands [L=2,9-(ArNCH)2C12H6N2] were synthesized. The solid-state structures of 4 and 7 have been determined by single-crystal X-ray diffraction study. Treatment of the complexes LMX2 with methylaluminoxane (MAO) leaded to activate ethylene as oligomerization catalysts.