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IOP Publishing, Journal of Physics: Conference Series, 3(568), p. 032011, 2014

DOI: 10.1088/1742-6596/568/3/032011

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Cryogen free cryostat for neutron scattering experiments

Journal article published in 2014 by Oleg Kirichek, R. B. E. Down, P. Manuel ORCID, J. Keeping, Z. A. Bowden
This paper is made freely available by the publisher.
This paper is made freely available by the publisher.

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Abstract

Most very low temperature (below 1K) experiments at advanced neutron facilities are based on dilution and 3He refrigerator inserts used with Orange cryostats, or similar systems. However recent increases in the cost of liquid helium caused by global helium supply problems, has raised significant concern about the affordability of such cryostats. Here we present the design and test results of a cryogen free top-loading cryostat with a standard KelvinoxVT® dilution refrigerator insert which provides sample environment for neutron scattering experiments in the temperature range 35 mK – 300 K. The dilution refrigerator insert operates in a continuous regime. The cooling time of the insert is similar to one operated in the Orange cryostat. The main performance criteria such as base temperature, cooling power, and circulation rate are compatible with the technical specification of a standard dilution refrigerator. In fact the system offers operating parameters very similar to those of an Orange cryostat, but without the complication of cryogens. The first scientific results obtained in ultra-low temperature neutron scattering experiment with this system are also going to be discussed.