Published in
Taylor and Francis Group, High Pressure Research, 4(33), p. 720-724
DOI: 10.1080/08957959.2013.819098
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Preparation of a macrocrystalline pressure calibrant SrB4O7:Sm2+suitable for the HP-HTpowder diffraction
Journal article published in 2013 by
Sergey V. Rashchenko 
,
Anna Y.-U. Likhacheva,
Tatyana B. Bekker
,
Anna Y.-U. Likhacheva,
Tatyana B. Bekker
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Abstract
A new simplified synthesis of monocrystalline chips of SrB4O7: Sm2+ pressure calibrant, well-suited for the diamond anvil cell (DAC) powder diffraction experiments, is proposed. It consists of ordinary solid-state synthesis of fine-grained SrB4O7: Sm2+ and subsequent annealing near melting temperature. The obtained material was characterized and tested in HP-HT DAC experiment.