Published in
Wiley, Angewandte Chemie International Edition, 6(51), p. 1432-1436, 2011
Wiley, Angewandte Chemie, 6(124), p. 1461-1465, 2011
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Selenenylsulfide-Linked Homogeneous Glycopeptides and Glycoproteins: Synthesis of Human "Hepatic Se Metabolite A"
Journal article published in 2011 by
Omar Boutureira,
Gonçalo J. L. Bernardes 
,
Marta Fernández-González ,
Daniel C. Anthony,
Benjamin G. Davis
,
Marta Fernández-González ,
Daniel C. Anthony,
Benjamin G. Davis
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Abstract
Introducing selenium: The synthesis and full characterization of human hepatic Se metabolite A has been accomplished by using a robust, efficient, and Cys-specific selenenylation protocol (see scheme; NaPi=sodium phosphate). The selenenylsulfide linkage is sufficiently stable to allow quantification of Se-containing glycoconjugates in biological fluids by using atomic detection methods.