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Wiley, Journal of Inorganic and General Chemistry, 6(636), p. 1090-1094, 2010
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Reactions of Distibanes with [Fe2(CO)9]: Synthesis, Structure and DFT Calculations of [(Et2Sb)4Fe4(CO)14], [(nPr2Sb)4Fe3(CO)10], [{(Me3SiCH2)2Sb}4Fe2(CO)6], and [2-(Me2NCH2)C6H4SbFe2(CO)8]
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Abstract
The iron complexes [(Et2Sb)4Fe4(CO)14] (1), [(nPr2Sb)4Fe3(CO)10] (2), [{(Me3SiCH2)2Sb}4Fe2(CO)6] (3), and [2-(Me2NCH2)C6H4SbFe2(CO)8] (4) were prepared by reactions of distibanes with Fe2(CO)9. Compounds 1–4 were characterized by X-ray diffraction, 1H NMR and IR spectroscopy as well as mass spectrometry; complex 1 was additionally characterized by density functional calculations.