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Wiley, Journal of Microscopy, 3(223), p. 216-219, 2006

DOI: 10.1111/j.1365-2818.2006.01623.x

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Characterization of nanostructured binary molybdenum oxide catalyst precursors for propene oxidation

Journal article published in 2006 by J. B. Wagner ORCID, N. D. Othman, D. S. Su, S. B. A. Hamid ORCID, R. Schlögl
This paper is made freely available by the publisher.
This paper is made freely available by the publisher.

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Abstract

High-resolution transmission electron microscopy characterization of molybdenum oxide catalyst precursors is carried out for a better understanding of the mechanisms leading to the active catalytic material. The precipitated material consists of both large-unit cell crystals and randomly orientated clusters on a 3-5 nm scale. The crystalline clusters are embedded in non-crystalline material, preventing the formation of large well-defined inactive orthorhombic MoO(3) crystals during activation of the catalyst material.