Elsevier, Chemical Physics Letters, 3-4(293), p. 173-179
DOI: 10.1016/s0009-2614(98)00761-1
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We excite triple quantum coherence between carbon-13 nuclei in magic-angle-spinning solid state NMR, using a C7 pulse sequence applied to transverse -magnetization. Experimental results on a powder of 98% labelled l-alanine are in good agreement with analytical solutions and exact numerical simulations. We achieve a triple-quantum filtering efficiency of around 8% for the central site in the three-spin topology.