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American Chemical Society, Organic Letters, 19(13), p. 5270-5273, 2011

DOI: 10.1021/ol202140y

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Concise Asymmetric Total Synthesis of 9-epi-Sessilifoliamide J

Journal article published in 2011 by Shi-Chuan Tuo, 黄培强, Jian-Liang Ye, Ai-E. Wang, Su-Yu Huang, Pei-Qiang Huang ORCID
This paper was not found in any repository; the policy of its publisher is unknown or unclear.
This paper was not found in any repository; the policy of its publisher is unknown or unclear.

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Abstract

A 10-step asymmetric synthesis of 9-epi-sessilifoliamide J (20), together with sessilifoliamide J (6), has been accomplished from the key chiral building block 11 via a threo-selective vinylogous Mannich reaction and a Ley oxidation-SmI(2)-mediated coupling lactoniation. The absolute configuration of the natural sessilifoliamide J was established. ; National Basic Research Program (973 Program) of China[2010CB833200]; NSF of China[20832005, 21072160]; NSF of Fujian Province of China[2011J01056]