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International Union of Crystallography, Acta Crystallographica Section E: Structure Reports Online, 1(63), p. o197-o199, 2006

DOI: 10.1107/s1600536806052202

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Methyl 4-chloro-3,5-di-p-tolyl-1H-pyrrole-2-carboxylate dichloromethane hemisolvate

Journal article published in 2006 by Mg Gardiner ORCID, Sarah Ng, Roderick C. Jones, M. Ng, Ja Smith
This paper is made freely available by the publisher.
This paper is made freely available by the publisher.

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Abstract

Recently, we have developed a synthetic procedure that allows the controlled formation of mono- and diarylpyrroles by chemoselective Suzuki–Miyaura coupling (Smith et al., 2006). The key to the method was using chloride as a blocking group which is not very reactive for cross-coupling, and then its removal by catalytic hydrogenation.