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American Chemical Society, Journal of the American Chemical Society, 8(130), p. 2412-2413, 2008

DOI: 10.1021/ja710557t

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A High-Resolution43Ca Solid-State NMR Study of the Calcium Sites of Hydroxyapatite

Journal article published in 2008 by Danielle Laurencin, Alan Wong, John V. Hanna, Ray Dupree ORCID, Mark E. Smith
This paper was not found in any repository; the policy of its publisher is unknown or unclear.
This paper was not found in any repository; the policy of its publisher is unknown or unclear.

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Abstract

High resolution Ca-43 solid-state NMR studies of hydroxyapatite (Ca-10(PO4)(6)(OH2)) were performed at 14.1 T. The two crystallographically distinct calcium sites were unequivocally resolved by a triple-quantum magic angle spinning experiment, and the unambiguous assignment of the signals was possible using H-1-Ca-43 rotational echo double resonance and H-1-Ca-43 cross polarization magic angle spinning experiments.