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American Chemical Society, Journal of Organic Chemistry, 3(68), p. 1158-1160, 2002

DOI: 10.1021/jo026407z

Wiley-VCH Verlag, ChemInform, 25(34), 2003

DOI: 10.1002/chin.200325061

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Direct Conversion of Aldehydes to Amides, Tetrazoles, and Triazines in Aqueous Media by One-Pot Tandem Reactions

Journal article published in 2002 by Jim-Min Fang, Jiun-Jie; Fang Jim-Min Shie ORCID
This paper was not found in any repository, but could be made available legally by the author.
This paper was not found in any repository, but could be made available legally by the author.

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Abstract

A variety of aldehydes reacted with iodine in ammonia water at room temperature to give the nitrile intermediates, which were trapped by addition of hydrogen peroxide, sodium azide, or dicyandiamide to produce their corresponding amides, tetrazoles, and 1,3,5-triazines in modest to high yields. The one-pot tandem reactions were conducted in water media, and the products were obtained simply by extraction or filtration.