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Pt nanocubes/rGO in one pot: Pt nanocubes/rGO hybrids are successfully synthesized via a facile one-pot approach. The resultant Pt nanocubes/rGO hybrid exhibits enhanced catalytic activity and excellent electrochemical stability in comparison with commercial Pt/CB electrocatalysts, which can be ascribed to the abundant Pt(100) surface and its uniform distribution on rGO.