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Material identification is playing an increasingly important role in various sectors such as industry, petrochemical, mining, and in our daily lives. In recent years, material identification has been utilized for security checks, waste sorting, etc. However, current methods for identifying materials require direct contact with the target and specialized equipment that can be costly, bulky, and not easily portable. Past proposals for addressing this limitation relied on non-contact material identification methods, such as Wi-Fi-based and radar-based material identification methods, which can identify materials with high accuracy without physical contact; however, they are not easily integrated into portable devices. This paper introduces a novel non-contact material identification based on acoustic signals. Different from previous work, our design leverages the built-in microphone and speaker of smartphones as the transceiver to identify target materials. The fundamental idea of our design is that acoustic signals, when propagated through different materials, reach the receiver via multiple paths, producing distinct multipath profiles. These profiles can serve as fingerprints for material identification. We captured and extracted them using acoustic signals, calculated channel impulse response (CIR) measurements, and then extracted image features from the time–frequency domain feature graphs, including histogram of oriented gradient (HOG) and gray-level co-occurrence matrix (GLCM) image features. Furthermore, we adopted the error-correcting output code (ECOC) learning method combined with the majority voting method to identify target materials. We built a prototype for this paper using three mobile phones based on the Android platform. The results from three different solid and liquid materials in varied multipath environments reveal that our design can achieve average identification accuracies of 90% and 97%.