Published in

International Union of Crystallography, Journal of Applied Crystallography, 4(54), p. 1268-1270, 2021

DOI: 10.1107/s1600576721006671

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A simple gas introduction system for cryogenic powder X-ray diffraction

Journal article published in 2021 by Robert Hodyss, Tuan H. Vu ORCID, Mathieu Choukroun, Morgan L. Cable ORCID
This paper was not found in any repository, but could be made available legally by the author.
This paper was not found in any repository, but could be made available legally by the author.

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Abstract

A simple system is described for the introduction of gases into standard X-ray diffraction capillaries mounted in situ in the X-ray beam of laboratory X-ray diffraction instruments. This system retains many of the advantages of the standard Norby cell, but does not require custom machining and has less stringent space restrictions. The system has been used to study the crystallization and interaction of volatile organics at cryogenic temperatures, but gas–solid interactions could also be studied at elevated temperatures using this approach.