Published in

Nature Research, Scientific Reports, 1(11), 2021

DOI: 10.1038/s41598-021-97112-x

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Π-GISANS: probing lateral structures with a fan shaped beam

Journal article published in 2021 by Alexei Vorobiev, Nicolò Paracini ORCID, Marité Cárdenas, Max Wolff
This paper is made freely available by the publisher.
This paper is made freely available by the publisher.

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Abstract

AbstractWe have performed grazing incidence neutron small angle scattering using a fan shaped incident beam focused along one dimension. This allows significantly reduced counting times for measurements of lateral correlations parallel to an interface or in a thin film where limited depth resolution is required. We resolve the structure factor of iron inclusions in aluminium oxide and show that the ordering of silica particles deposited on a silicon substrate depends on their size. We report hexagonal packing for 50 nm but not for 200 nm silica spheres deposited by a modified Langmuir-Schaefer method on a silicon substrate. For the 200 nm particles we extract the particles shape from the form factor. Moreover, we report dense packing of the particles spread on a free water surface. We name this method π-GISANS to highlight that it differs from GISANS as it gives lateral information while averaging the in-depth structure.