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Published in

Elsevier, International Journal of Inorganic Materials, 5-6(1), p. 351-355

DOI: 10.1016/s1466-6049(99)00050-1

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Thermal treatment of a Y-123 precursor prepared using the hydroxide co-precipitation method

This paper was not found in any repository, but could be made available legally by the author.
This paper was not found in any repository, but could be made available legally by the author.

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Abstract

A Y-123 precursor has been obtained using the hydroxide co-precipitation method. The influences of the calcination time and temperature (with and without sintering and annealing) on the formation of the superconducting phase, YBa2Cu3O7-delta, are examined using XRD and T-c measurements. A comparison between the co-precipitated hydroxide precursor and the conventional dry precursor, obtained by mixing oxides acid carbonates, is made. It shows that thermal treatment of the hydroxide precursor at 750 degrees C already gives a superconductor, while the oxide-carbonate precursor is only superconducting after thermal treatment at 850 degrees C. (C) 1999 Elsevier Science Ltd. All rights reserved.