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Published in

International Union of Crystallography, Journal of Applied Crystallography, 5(55), p. 1255-1266, 2022

DOI: 10.1107/s160057672200766x

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HTD2: a single-crystal X-ray diffractometer for combined high-pressure/low-temperature experiments at laboratory scale

This paper was not found in any repository, but could be made available legally by the author.
This paper was not found in any repository, but could be made available legally by the author.

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Postprint: archiving allowed
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Data provided by SHERPA/RoMEO

Abstract

High-pressure (HP) X-ray diffraction experiments at low temperature (LT) require dedicated instruments as well as non-standard sample environments and measuring strategies. This is especially true when helium cryogenic temperatures below 80 K are targeted. Furthermore, only experiments on single-crystalline samples provide the prerequisites to study subtle structural changes in the p–T phase diagram under extreme LT and HP conditions in greater detail. Due to special hardware requirements, such measurements are usually in the realm of synchrotron beamlines. This contribution describes the design of an LT/HP diffractometer (HTD2) to perform single-crystal X-ray diffraction experiments using a laboratory source in the temperature range 400 > T > 2 K while applying pressures of up to 20 GPa.