Published in
Royal Society of Chemistry, Chemical Science, 9(13), p. 2591-2603, 2022
DOI: 10.1039/d1sc06060k
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Solid-state <sup>17</sup>O NMR study of α-d-glucose: exploring new frontiers in isotopic labeling, sensitivity enhancement, and NMR crystallography
Journal article published in 2022 by
Jiahui Shen,
Victor Terskikh 
,
Jochem Struppe ,
Alia Hassan,
Martine Monette,
Ivan Hung ,
Zhehong Gan ,
Andreas Brinkmann ,
Gang Wu
,
Jochem Struppe ,
Alia Hassan,
Martine Monette,
Ivan Hung ,
Zhehong Gan ,
Andreas Brinkmann ,
Gang Wu
This paper is made freely available by the publisher.
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Abstract
We report the first “total synthesis” of 17O-labeled d-glucose and its solid-state 17O NMR characterization with unprecedented sensitivity and resolution.